Analysis for Gold, Platinum Group Metals and Other Elements

Aqua Regia Digestion

Aqua regia will digest most rock types, however silicates and refractory minerals will remain essentially un-dissolved.

We offer two options -

Digestion B (10g charge)

Our proven technique used extensively at Genalysis for the past 25 years, for gold and base metals. The digested and leached sample is vacuum filtered and accurately diluted to volume.

Digestion cost (10g charge - gold only required)$3.80 sample
Digestion cost (10g charge - gold and other elements required)$4.50 sample

Digestion B25 (25g charge)

For this option the digested and leached sample is vacuum filtered and accurately diluted to volume.

Digestion cost (25g charge – suitable for gold only)$4.80 sample
Digestion cost (25g charge – gold and other elements required)$5.50 sample

Digestion B5 (50g charge)

This option involves arresting the digest and diluting to volume in the beaker. Any insoluble residue remains in situ. Base metals based on this technique are not as efficiently recovered and duplication is poor.

Digestion cost (50g charge – suitable for gold only)$6.30 sample
Digestion cost (50g charge – gold and other elements required)$7.00 sample

Digestion RB

Aqua regia digest after pre-roasting (ashing) to remove graphitic and other organic material. (NB some analytes may be lost during roasting.) 10g charge only.

Pre-roast and Digestion cost (gold only required)$5.80 sample
Pre-roast and Digestion cost (gold and other elements required)$6.50 sample

Samples submitted for ppb detection of gold are digested in our completely separate and dedicated laboratory away from samples submitted for ppm detection.

Elements by solvent extraction and enhanced sensitivity graphite furnace AAS [EETA]
Method code B/EETA; B25/EETA; B5/EETA; RB/EETA

Au(0.1ppb)$7.00

Elements by solvent extraction and graphite furnace AAS [ETA]
Method code B/ETA; B25/ETA; B5/ETA; RB/ETA

Au(1ppb)$4.50

Elements by solvent extraction and flame AAS [SAAS]
Method code B/SAAS; B25/SAAS; B5/SAAS; RB/SAAS

Au(0.01)$1.20

Elements by flame AAS
Method code B/AAS; B25/AAS; B5/AAS; RB/AAS

Ag (0.1) As (10) Bi (2) Cd (0.1) Co (1) Cu (1) Mn (1) Ni (1) Pb (1) Sb (2) Te (2) Tl (2) Zn (1) $1.20 each
Cr (1) Fe (0.01%) Mo (2) $1.80 each
Ca (0.1%) Mg (0.1%)$3.00 each

Elements by OES
Method code B/OES; B25/OES; B5/OES; RB/OES
Ag (0.5) Al (20) As (2) Ba (2) Bi (10) Ca (0.01%) Cd (0.5)
Co (1) Cr (2) Cu (1) Fe (0.01%) K (20) Mg (0.01%) Mn (1)
Mo (2) Ni (1) P (20) Pb (2) Sb (10) Sc (1) Sr (1) Te (5) Ti (5) V (2) Zn (1)

first element$5.00
subsequent elements$0.50 each

Elements by enhanced sensitivity OES [EOES]
Method code B/EOES; B25/EOES; B5/EOES; RB/EOES
Ag (0.1) Bi (1) Cd (0.1) Mo (1) Pb (1) Sb (1) Te (1) Tl (1) W (2)

first element$5.00
subsequent elements$0.70 each

(If both "standard" and "enhanced" OES elements are reported, then the "first element" cost for the "enhanced" OES elements does not apply).

Elements by MS
Method code B/MS; B25/MS; B5/MS; RB/MS
Ag (0.01) As (0.5) Au (1ppb) Ba (1) Be (0.05) Bi (0.01) Cd (0.05) Ce (0.01) Co (0.1) Cs (0.002) Dy (0.01) Er (0.01) Eu (0.01) Ga (0.05) Gd (0.01) Hf (0.01) Ho (0.01) In (0.01) La (0.01) Li (0.1) Mo (0.1) Nb (0.02) Nd (0.01) Pb (1) Pd (10ppb) Pr (0.005) Pt (5ppb) Rb (0.02) Re (0.01) Sb (0.02) Se (1) Sm (0.01) Sn (0.05) Sr (0.02) Ta (0.01) Tb (0.005) Te (0.05) Th (0.01) Tl (0.01) Tm (0.01) U (0.01) W (0.05) Y (0.02) Yb (0.01) Zr (0.1)

first element$7.00
subsequent elements$0.70 each

Elements by enhanced sensitivity MS [EMS]
Method code B/EMS; B25/EMS; B5/EMS; RB/EMS
As (0.1) Se (0.2)

first element$7.00
second element$0.70

Digestion FA

Lead collection fire assay using carefully selected fluxes specially formulated for the mineralogy of each sample type. Samples submitted for ppb detection of gold (and/or platinum and palladium) are fused in our dedicated low level furnace. Some reduction in charge weight may be necessary for difficult sample matrices. Prices exclude the lead waste disposal levy.

Digestion cost (Standard Fusion – 50g charge) Method code FA50/ $8.10 sample
Digestion cost (Standard Fusion – 25g charge) Method code FA25/ $7.50 sample
Digestion cost (Metallurgical/Mill) Method code FA25M/ $9.40 sample
Digestion cost (Concentrate) Method code FA25C/ $11.20 sample
Digestion cost (Shipment Samples) Method code FA25S/ $12.30 sample

Elements by flame AAS
Method code FA/AAS

Au (0.01)$1.20

Elements by solvent extraction & flame AAS [SAAS]
Method code FA/SAAS

Au (1ppb)$3.60

Elements by MS
Method code FA/MS
Au (1ppb) Pd (1ppb) Pt (1ppb)

first element$7.00
subsequent elements$0.70 each
Waste Disposal Levy (not subject to any discount)$0.50 sample

Digestion NiS

Nickel sulfide collection fire assay is formulated for the total recovery of all the platinum group elements. Some reduction in charge weight may be necessary for difficult sample matrices

Digestion cost (25g charge)$52.00 sample

Elements by MS
Method code NIS/MS
Au (5ppb) Ir (2ppb) Os (2ppb) Pd (2ppb) Pt (2ppb) Rh (2ppb) Ru (2ppb)

first element$11.00
subsequent elements$2.00 each
Waste Disposal Levy (not subject to any discount)$0.50 sample

Screen Fire Assays

A specified weight (usually 500g to 1kg) is split from the bulk pulp which is then re-pulverised to (hopefully) ensure oversize portion is not excessive. This sub-sample is then sieved wet or dry through a specified mesh size nylon cloth. The coarse fraction is weighed and the total coarse fraction including nylon cloth is fired in a new pot and the micrograms of gold determined. The fines are homogenised and duplicate portions fire assayed and the gold determined in ppm. The "true" or "weighted mean" result is then calculated.

Special pre-preparation of samples prior to screen fire assay$5.00 sample
The most common option is for 1kg sample, dry sieved through 150 micron cloth, and duplicate 25g fire assays of the fines.$50.00 sample
Another option is for 1kg sample, dry sieved through 100 micron cloth, and duplicate 25g fire assays of the fines.$60.00 sample
Alternatively, 1kg sample, dry sieved through 75 micron cloth, and duplicate 25g fire assays of the fines.$100.00 sample
The above prices allow for a single pot fire of oversize. Additional oversize firing.$12.10 sample
Other optionsprice on application
Also applicable to silver and platinum/palladiumprice on application.
Waste Disposal Levy (not subject to any discount)$1.50 sample

LeachWELL™ Accelerated Cyanide Leach

4 hour leach using 10g LeachWELL™ tablet. Not practicable for clay rich samples.

200g leach$7.80 sample
400g leach$8.80 sample
1000g leach (two tabs)$13.80 sample

Elements by Solvent Extraction & flame AAS [SAAS]
Method code LW200/SAAS; LW400/SAAS; LW1000/SAAS

Au (0.01)$1.20

Elements by flame AAS
Method code LW200/AAS; LW400/AAS; LW1000/AAS

Ag (1)$1.20
Filtration to recover clear liquor for analysis (if required)$6.00 sample

Tail recovery, entire tail washed, reground and 25g Fire Assay

LW200$22.00 sample
LW400$22.00 sample
LW1000'$25.00 sample

Waste Disposal Levy (not subject to any discount)

LW200$0.50 sample
LW400$1.00 sample
LW1000$2.00 sample

Bulk Cyanide Leach - Low Level Gold (BLEG)
24 hour tumble leach at standard conditions formulated for oxidised surface samples containing little organic matter. Usually performed on minus 2mm unprepared sample.

0.1kg leach$6.50 sample
0.5kg leach$8.80 sample
1.0kg leach$10.80 sample
2.0kg leach$12.80 sample
4.0kg leach$17.80 sample

Elements by MS
Method codeCN.1/MS; CN.5/MS; CN1/MS; CN2/MS; CN4/MS
Ag (0.1ppb) As (0.02) Au (0.01ppb) Bi (0.1 ppb) Cd (0.1ppb) Co (0.001) Cu (0.01)
Hg (0.5ppb) Mo (0.1ppb) Ni (0.01) Pd (0.1ppb) Pt (0.1ppb) Zn (0.05)

first element$7.00
subsequent elements$0.70 each
Hg as a subsequent element$1.50
Waste Disposal Levy (not subject to any discount)$0.50 sample